Master’s studies

Syllabus for NMR Spectroscopy II

NMR-spektroskopi II

Syllabus

  • 5 credits
  • Course code: 1KB470
  • Education cycle: Second cycle
  • Main field(s) of study and in-depth level: Chemistry A1F
  • Grading system: Fail (U), 3, 4, 5.
  • Established: 2013-03-21
  • Established by: The Faculty Board of Science and Technology
  • Revised: 2016-04-20
  • Revised by: The Faculty Board of Science and Technology
  • Applies from: week 30, 2016
  • Entry requirements: Participation in NMR Spectroscopy I, 5 credits, or Spectroscopic Methods for Organic Chemistry, 7.5 credits, or Organic Chemistry II, 15 credits, including practical use of NMR equipment.
  • Responsible department: Department of Chemistry - BMC

Learning outcomes

After successful completion of the course, the participant should have the ability to:

  • describe the basic function of some common pulse sequences
  • optimise the key parameters in these pulse sequences and be able to perform simple parameter calibrations
  • quantify the composition of mixtures
  • independently plan and carry out structural determination of more complex organic compounds (molecular weight up to approx. 500 Da) using appropriate NMR experiments efficiently
  • discuss the impact of dynamics in organic and organometallic compounds on their NMR spectra
  • plan and implement experiments relevant for the course, interpret and document their results

Content

The vector model and its relation to pulse sequences. Function of pulse sequences. Parameter calibration and optimisation. Structural determination of a series of organic molecules of increasing complexity. Spectra of organometallic compounds, fluxionality. Molecular interaction and its effect on NMR spectra.

Instruction

Seminars and laboratory exercises. Laboratory work and related tutorials and presentations are compulsory.

Assessment

Written examination at the end of the course, laboratory exercises and related written reports and oral presentations. The examination and oral presentations are equivalent to 2 credits. The laboratory exercises and related reports are equivalent to 3 credits.

Reading list

Applies from: week 31, 2016

  • Claridge, Timothy D. W. High-resolution NMR techniques in organic chemistry

    2. ed.: Amsterdam: Elsevier, cop. 2009

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