Electron Microscopy and Nanoengineering

Quantitative electron microscopic analysis of materials that take their functionality from individual nano-objects.

The Elmin research group, is dedicated to the quantitative electron microscopy analysis of materials that take their functionality from single nano-objects down to single atoms as well as to the fabrication of nanomaterials and nano-devices for environmental and health applications.

Our research is driven by the one-nano down to one-atom vision

Transmission electron microscopy methods are developed and applied as a quantitative tools for down to atomic scale analysis. The establishment of structure-property relations is one of the main topics of the electron microscopy activity. Techniques currently developed are related to electron energy loss spectroscopy (EELS), 3D electron tomography, electron magnetic circular dichroism (EMCD), fluctuation electron microscopy (FEM), strain analysis and quantitative EDS analysis. The research is carried out at resolutions down to 1.3 Å on the TEM at the Ångström Laboratory and for need of higher resolution with our friends and partners. We have developed a cryo-method for FIB-lift-out of frozen samples for analysis of interfaces between hard and soft matter in the TEM.

Two nanomaterials platforms

We have developed two nanomaterials platforms for fundamental and applied studies of nanomaterials properties. The first platform is nano-electrode based, where the electrodes are bridged by chains of alternating molecules and nanoparticles. A reproducible molecular electronics platform has thus been established. The junctions have suchhigh order that we can observe molecular vibrational signatures of the molecules in IETS spectra. More recently, we have observed gas sensing signatures with the same platform.

Functionalisation of graphene is essential to bring graphene into applications. Using electron and ion beam microscopes, we functionalise graphene in order to maintain excellent electrical properties and to modify chemical, sensing and electrical properties. In our research on graphene, we modify graphene with precision on the nanometer scale, both by inserting defects as well as by functionalizing through physical and chemical routes. We have explored modification of electronic structure, electrical properties and sensing properties of graphene.

The Elmin-lab

In addition to Nano Synthesis/Analysis methods and equipments available at Micro Structure Laboratory, we at Elim-lab have developed a lab equipped with high-end electrical characterization instruments.

Inclusion of Multimode 8 AFM has enhanced our competence in atomic force microscopy for property measurement and material characterization.

These instruments are available in the Elmin laboratory

The electron microscope is a versatile tool used to obtain structural, magnetic and electronic information. Different imaging, reciprocal space as well as spectroscopic techniques are applied to retrieve these materials properties with a spatial resolution down to 1 Ångström. Focussed ion and electron beams are used to nano-structure matter.

Electron microscopy proactively contributes to the search of novel materials both in applied and basic studies. In most modern hard and biological materials the study of structural and electronic properties on the atomic scale is key for the understanding of mesoscopic and macroscopic properties. Several techniques in electron microscopy shade light in materials properties on this length scale. Structural imaging enables us to detect atomic configurations at interfaces or in nanoparticles. Nanoparticles, first used to colorize medieval church windows, nowadays have a broad range of applications. Using high resolution electron microscopy, we contribute to the understanding the fundamental interplay between particle structure and physical properties. Thus these particles can be engineered for use in applications ranging from catalysers over light emitters to cancer therapy. The distribution of elements in a material or in a tissue can often not be derived from a study of the crystal structure alone. Spectroscopic methods in the electron microscope are not only used to identify the local position of chemical elements with subnanometer resolution but also to study their electronic properties. The electron beam in the microscope also interacts with magnetic fields in the sample. In fact, by using the techniques of Lorentz microscopy and electron holography, we can visualise magnetic field lines and domains.

The use of focussed electron and ion beams allows us to structure matter on a length scale of 10nm to some 100nm. Particle assisted structuring contains several approaches such as sputtering, etching, deposition as well as materials transformations. Using these instruments, nanopillars can be grown that are inserted into magnetic force microscopes. The development of ion beam assisted deposition enables us to contact device elements or nanowires. By focussed ion beam sputtering, structures such as electrodes, trenches and fresnel lenses can be created. The intimate link between electron microscopy and advanced focussed ion beam techniques (FIB) is the capacity of the FIB to prepare electron transparent samples on well defined sites, i.e. in a device.

Klaus Leifer
Professor

Ling Xie
Researcher

Hasan Ali
Post Doc

Sharath Kumar
PhD student

Alumni

Thomas Thersleff
Post Doc

Anumol Ashokkumar
Post Doc

Syed Hassan M. Jafri
Post Doc

Ling Xie
PhD student

Hu Li
PhD student

Ishtiaq Hassan Wani
PhD student

Yuanyuan Han
PhD student

Hasan Ali
PhD student

Farnaz Ghajeri
PhD student

Luimar Correa Filho
PhD student

Linus Schönström
Master student

Mikael Anttila-Eriksson
Master Student

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