High-current implanter with keV Ions

Big square machine

For ion implantation and ion beam analysis with keV ions, an accelerator platform is available that can produce ion beams up to 350 kV from a substantial fraction of all elements in the periodic table.

For ion implantations as well as ion beam analysis methods using keV ions, the Tandem laboratory features a Danfysik 1090 accelerator platform. The machine is equipped with a highly versatile ion source that allows us to produce ion beams from almost all elements of the periodic table for a wide range of applications. The ions are accelerated with up to 350 kV and steered into one of three beamlines for different applications.

  • Ion Implantations. The first beamline is dedicated to implantations and irradiations. Beam currents of up to a few mA enable high-dose implantations even on large targets.
  • ToF-MEIS System. The second beamline consists of our unique Time-of-Flight Medium-Energy Ion Scattering (ToF-MEIS) system, used for high-resolution depth profiling and crystallography of thin films.
  • Multifunctional Scattering Chamber. The third beamline extends to a multipurpose scattering chamber. Most prominently, the set-up allows to depth-profile ¹¹B and ¹⁸O using nuclear reactions.

 

Beamline 1: Implantations

Final station of the implantation beamline. A man in protective gear is installing wafers.

A wide range of elements is available for ion implantation at energies up to 350 keV.

Ion implantation is routinely used by both academic researchers and industry for numerous applications, for example in microchip manufacturing.

The Tandem Laboratory’s implantation facility is the only academically operated and openly accessible one of its kind in Sweden. Researchers and companies without their own implanter can apply for beam time.

The target chamber is accessed through a cleanroom environment to ensure ultra-clean surfaces during sample preparation and mounting.

Wide range of implantation elements

The Tandem Laboratory’s ion implanter provides a broad selection of available source materials to meet requests for various ion species. Examples of available ions include those commonly used in semiconductor dopants (B, BF₂, Al, P, As, and others), various metals (e.g. Fe, W), as well as light and heavy noble gases.

Adjustable irradiation flux, dose, and charge state

We can adjust particle flux and dose, and deliver either singly or doubly charged ions. The latter enables ion energies of up to 700 keV at maximum acceleration voltage. Due to the high achievable beam current (up to several mA), implantation at very high doses is possible. See the publication below for an example.

  • Wide range of ion species.
  • Deceleration unit in the beamline to allow for ion energies down to 2 keV.
  • Beam scanning and focussing for homogeneous exposure over large areas.
  • Maximum target size: ∅ 6''. Standard sample holder available for 2'', 4'' and 6'' samples.
  • Water cooling of the sample holder.
  • Hot implantations at temperatures up to 650°C possible.
  • Adjustable incident angle between the ion beam and the target surface.

Beamline 2: The ToF-MEIS System and High-resolution depth profiling of thin films

Experimental set-up in a laboratory that consists of several vacuum chambers. A man is shown on the right. He adjusts something on top of the front chamber.

The Time-of-Flight Medium-Energy Ion Scattering (ToF-MEIS) system is a developed at the Tandem Laboratory using pulsed keV ion beams enabling in-situ studies of thin layers.

Designed by researchers at the Tandem Laboratory, the Time-of-flight medium-energy ion scattering (ToF-MEIS) system combines pulsed keV ion beams with advanced detection technology.

This unique equipment has been developed for non-destructive, high-depth-resolution analysis of the chemical composition and crystallographic structure of thin layers.

In this beamline, the keV ion beam from the implantation platform is divided into short pulses approximately 1 nanosecond in duration. This allows for high-resolution energy measurements, beneficial both for fundamental research on ion-solid interactions and for depth-resolved studies of materials at the nanometre scale.

Angle-resolved measurements

The scattering chamber features two detectors. The first detector is movable and can be positioned at any scattering angle for measurements in different geometries (backscattering, forward scattering, and transmission geometry). Its large area enables short measurement times as well as angle-resolved measurements and imaging of crystal structures.

Sub-nanometre depth resolution

The second detector is fixed at a longer distance from the sample, providing improved time resolution corresponding to a depth resolution of below one nanometre. The detector type used is sensitive sensitive not only to ions but also capable of detecting neutral atoms, electrons, and photons.

The ToF-MEIS system is complemented by a sample preparation chamber allowing fabrication of thin films and preparation of surfaces for in-situ studies ofof surface and near-surface phenomena.

  • Non-destructive measurement technique due to use of a pulsed ion beam.
  • Additional drift tube buncher can be used to decrease pulse width even further to about 0.3 ns.
  • Sample mounted on 6-axes goniometer allowing for 3 translational and 3 rotational movements.
  • Sample holder for transmission experiments on self-supporting foils available.
  • In-situ annealing at up to 600°C.
  • Possibility to vary the potential of the sample holder between -500 V and 500 V, thereby allowing for the detection of low-energy secondary ions and electrons.
  • Two microchannel plate (MCP) detectors coupled with two delay lines each to record particle energy as well as position.
  • First detector: rotatable around the scattering point with a large solid angle of 0.13 sr.
  • Second detector: fixed at a backscattering angle of 135° at a distance of 1050 mm for enhanced energy resolution.
  • Possibility to measure the exit charge state during ion transmission experiments.
  • Charge deflection electrode in front of the second detector to separate neutrals from ions.
  • Chamber base pressure: <3 x 10-8 mbar.

  • 2 electron-beam evaporators, both capable of accommodating crucibles and rods, and operable at the same time for (co-)deposition of thin films.
  • 1 additional magnetron sputtering unit operable in DC or RF mode.
  • Gas inlet making reactive deposition processes possible.
  • keV sputter gun including Wien Filter.
  • Annealing of samples at temperatures up to 1200°C using an electron-beam heater.
  • Retractable button heater allowing for annealing at up to 500°C of even self-supporting targets.
  • Residual gas analysis during operation.

Beamline 3: Multifunctional Low-energy Ion Beam Analysis

Experimental set-up in a laboratory that consists of a beamline and a vacuum chamber. A man works on the vacuum chamber.

The multifunctional scattering chamber for sub-MeV ion beam analysis can, among other applications, be used for depth profiling of the isotopes ¹¹B and ¹⁸O via nuclear reactions.

This beamline is dedicated to sub-MeV ion beam analysis. Multiple detectors allow for near-surface materials characterisation with high resolution.

Isotope-selective studies of materials diffusion

A unique feature of this set-up is the usage of two nuclear resonances of keV protons: at 151 keV with ¹⁸O and at 163 keV with ¹¹B. By detecting the resulting alpha particles, these isotopes can be quantified depth-resolved permitting isotope-selective studies of materials diffusion. This capability has also been used to quantify boron in transition-metal borides, which are technologically relevant for coatings or as friction materials.

Other techniques available are high-solution backscattering spectrometry, also in combination with channelling, and low-energy PIXE for detection of elements as light as carbon.

  • Large-area (1200 mm2) passivated implanted planar silicon detector (PIPS) with absorbers to detect alpha particles from nuclear reactions.
  • Surface barrier detector (SBD) with cooled preamplifier electronics for high-resolution backscattering spectrometry. For protons and deuterons typical resolutions of 3 keV (FWHM) can be achieved.
  • Ultra-fast silicon drift detector (SDD) with very thin Be-window layer to detect characteristic X-rays from elements with Z ≥ 6.
  • Sample holder attached to remotely controlled 3-axes goniometer.
  • Beam currents up to µA achievable.
  • N2-trap to improve the chamber base pressure to <10-7 mbar.

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